Precision Chemistry
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Subjects / keywords: Science: Chemistry
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Precision Chemistry
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Subjects / keywords: chemistry, molecular engineering, nanotechnology, precision chemistry, synthesis, manufacturing; Science: Chemistry
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Open AccessA sustainable AQbD-based UHPLC–MS/MS method for the determination of hallucinogenic phenethylamines in urine
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A systematic Analytical Quality by Design (AQbD) approach was applied to the development and validation of a UHPLC–MS/MS method for the determination of hallucinogenic phenethylamine-derived novel psychoactive substanc...
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Material complementarioKnowledge mapping and bibliometric insights of scientific research on targeted protein degradation in oncology
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Abstract Background Disruption of cellular proteostasis leads to the accumulation and persistence of pathogenic proteins that drive oncogenesis. Key oncogenic and tumor suppressor proteins are frequently dysregulated in ...
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Material complementarioRadiotherapy meets anticancer metallodrugs
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Combined radiotherapy and chemotherapy remain central to cancer treatment, with metallodrugs – most notably platinum agents – playing indispensable roles in clinical regimens. However, systemic toxicity and limit...
LCC LCC:MedicineIdioma English
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Open AccessSpectral tuning of diamond photonic crystal slabs by deposition of a thin layer with silicon vacancy centers
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The controlled extraction of light from diamond optical color centers is essential for their practical prospective applications as single photon sources in quantum communications and as biomedical sensors in biosensing. ...
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Open AccessTrial watch: antibody-drug conjugates in cancer therapy
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Antibody-drug conjugates (ADCs) combine the target specificity of monoclonal antibodies with the cytotoxic potency of small-molecule payloads. In recent years ADCs have emerged as a clinically validated component of mode...
LCC LCC:Immunologic diseases. Allergy; TENDOk5lb3BsYXNtcy4gVHVtb3JzLiBPbmNvbG9neS4gSW5jbHVkaW5nIGNhbmNlciBhbmQgY2FyY2lub2dlbIdioma English
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Open AccessDetermination of sulphate for measuring magnesium sulphate in pharmaceuticals by flow analysis-fourier transforms infrared spectroscopy
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The viability of employing flow analysis coupled to Fourier transform infrared spectroscopy (FA-FTIR) as a useful tool for quantitative measuring of magnesium sulphate in pharmaceuticals was explored, developed and valid...
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Open AccessSensitive Spectrophotometric Method for Determination of Chloramphenicol in Pharmaceutical Preparations Using 7,7',8,8'-tetracyanoquinodimethane reagent
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Abstract A simple, sensitive and rapid spectrophotometric method for the determination of chloramphenicol in pure as well as in dosage form is described. The method is based on the reaction of reduced chloramphenicol wit...
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Open AccessCoupling MgSO4-assisted SALLE with a fluorimetric turn-off strategy for the determination of cinacalcet HCl in pharmaceutical and human matrices
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Abstract An innovative, sustainable analytical approach was developed by coupling an Epsom salt, E518 (magnesium sulfate)–facilitated salting-out assisted liquid–liquid extraction (SALLE) system with a safe molecular...
LCC LCC:Medicine; TENDOlNjaWVuY2U~Idioma English
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Open AccessDevelopment of a molecularly imprinted solid phase extraction sorbent for the selective removal of rivastigmine from serum samples
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A molecularly imprinted solid-phase extraction (MISPE) sorbent has been developed for the separation of RIV from serum sample. Molecularly imprinted polymer (MIP) was prepared via non-covalent imprinting technique using ...
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Open AccessSeparation and preconcentration of inorganic and organomercury species in water samples using a selective reagent and an anion exchange resin and determination by flow injection-cold vapor atomic absorption spectrometry
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An on-line inorganic (InHg) and organomercury (OrHg) species separation, preconcentration and determination system consisting of cold vapor atomic absorption spectrometry (CV-AAS) coupled to a flow injection (FI) method ...
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Material complementarioSolvent-based de-emulsification dispersive liquid-liquid microextraction coupled with UPLC-MS/MS for the fast determination of ultratrace levels of nitrated and oxygenated polycyclic aromatic hydrocarbons in environmental samples
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In this study, a new solvent-based de-emulsification dispersive liquid-liquid microextraction strategy followed by liquid chromatography-atmospheric pressure chemical ionization-tandem mass spectrometry has been develope...
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Material complementarioExtra Precision Glide: Docking and Scoring Incorporating a Model of Hydrophobic Enclosure for Protein−Ligand Complexes
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A novel scoring function to estimate protein-ligand binding affinities has been developed and implemented as the Glide 4.0 XP scoring function and docking protocol. In addition to unique water desolvation energy terms, p...
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Material complementarioAccurate Proteome-wide Label-free Quantification by Delayed Normalization and Maximal Peptide Ratio Extraction, Termed MaxLFQ
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Protein quantification without isotopic labels has been a long-standing interest in the proteomics field. However, accurate and robust proteome-wide quantification with label-free approaches remains a challenge. We devel...
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Material complementarioAn Empirical Method for Estimating the Degree of Crystallinity of Native Cellulose Using the X-Ray Diffractometer
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An empirical method for determining the crystallinity of native cellulose was studied with an x-ray diffractometer using the focusing and transmission techniques. The influence of fluctuations in the primary radiation an...
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Material complementarioEnzymatic Determination of Total Serum Cholesterol
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Abstract An enzymatic method is described for determination of total serum cholesterol by use of a single aqueous reagent. The method requires no prior treatment of sample and the calibration curve is linear to 600 mg/dl...
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Material complementarioTHE weighted histogram analysis method for free‐energy calculations on biomolecules. I. The method
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Article
Abstract The Weighted Histogram Analysis Method (WHAM), an extension of Ferrenberg and Swendsen's Multiple Histogram Technique, has been applied for the first time on complex biomolecular Hamiltonians. The method is pres...
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Material complementarioZener Model Description of Ferromagnetism in Zinc-Blende Magnetic Semiconductors
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Article
Ferromagnetism in manganese compound semiconductors not only opens prospects for tailoring magnetic and spin-related phenomena in semiconductors with a precision specific to III-V compounds but also addresses a question ...
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Página del recursoRapid Determination of Parabens in Water Samples by Ultra-high Performance Liquid Chromatography Coupled to Time of Flight Mass Spectrometry
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An analytical methodology has been developed and validated for the purpose of identifying and quantifying four parabens (methylparaben, ethylparaben, propylparaben and n-butylparaben) in water samples. The combination of...
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