A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route

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A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route

Suárez Gómez, A. et al · Springer · 2015

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Autor / responsable

Suárez Gómez, A. et al

Editorial

Springer

Año

2015

ISSN

0928-0707

ISSN

0928-0707

Idioma

Inglés

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In this work, we carried out the synthesis of lead(II) divanadate(V) by means of a soft chemistry reaction based on a sol–gel-derived route. The final organic precursor was heat treated (T = 400, 500, 600, 750 and 800 °C) and structurally analyzed for each temperature by taking into account the results of FTIR spectroscopy, synchrotron X-ray powder diffraction and X-ray absorption near-edge structure. As an overall result, we report a final compound with remarkable crystallographic and morphological qualities that seem to keep all its structural features in the temperature range 450–700 °C before the structure incongruently melts. As a highlight, the desired material was obtained following a highly reproducible, low-cost, low-temperature and quite straightforward chemical route. Besides, this synthesis route could also allow the appropriate integration of lead(II) divanadate(V) nanoparticles, or nanolayers, into more complex systems as well as the feasibility for being expanded to other materials. Fil: Suárez Gómez, A.. Universidad de Guadalajara; México Fil: Figueroa, Santiago Jose Alejandro. Brazilian Center of Energy and Materials; Brasil. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina

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APA 7

Suárez Gómez, A. E. A. (2015). A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route. http://hdl.handle.net/11336/41728

MLA

Suárez Gómez, A. et al. "A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route." 2015. http://hdl.handle.net/11336/41728.

Chicago

Suárez Gómez, A. et al. 2015. "A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route.". http://hdl.handle.net/11336/41728.

Harvard

Suárez Gómez, A. E. A. 2015, A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route, Springer, available at: http://hdl.handle.net/11336/41728 [Accessed 5 Aug. 2026].

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Título: A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route

Autor / colaboradores: Suárez Gómez, A. et al

Editorial: Springer

Año de publicación: 2015

ISSN: 0928-0707

ISSN: 0928-0707

Idioma: Inglés

Materias

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Divanadates; Synchrotron; Pb2v2o7; Sol Gel; Nanoparticles; https://purl.org/becyt/ford/2.10; https://purl.org/becyt/ford/2