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One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters

Castañar, Laura et al · American Chemical Society · 2016

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Author / responsible party
Castañar, Laura et al
Publisher
American Chemical Society
Year
2016
ISSN
0022-3263
ISSN
0022-3263
Language
English

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A novel approach for the fast and efficient structural discrimination of molecules containing multiple stereochemical centers is described. A robust J-resolved HSQC experiment affording highly resolved 1JCH/1TCH splittings along the indirect dimension and homodecoupled 1H signals in the detected dimension is proposed. The experiment enables in situ distinction of both isotropic and anisotropic components of molecules dissolved in compressed PMMA gels, allowing a rapid and direct one-shot determination of accurate residual dipolar coupling constants from a single NMR spectrum. Fil: Castañar, Laura. Universitat Autònoma de Barcelona; España Fil: García, Manuela Emila. University Of Carnegie Mellon; Estados Unidos. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto Multidisciplinario de Biología Vegetal. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas Físicas y Naturales. Instituto Multidisciplinario de Biología Vegetal; Argentina

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APA 7

Castañar, L. E. A. (2016). One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters. http://hdl.handle.net/11336/35193

MLA

Castañar, Laura et al. "One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters." 2016. http://hdl.handle.net/11336/35193.

Chicago

Castañar, Laura et al. 2016. "One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters.". http://hdl.handle.net/11336/35193.

Harvard

Castañar, L. E. A. 2016, One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters, American Chemical Society, available at: http://hdl.handle.net/11336/35193 [Accessed 7 Aug. 2026].

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Title
One-shot determination of residual dipolar couplings: application to the structural discrimination of small molecules containing multiple stereocenters
Author / contributors
Castañar, Laura et al
Publisher
American Chemical Society
Publication year
2016
ISSN
0022-3263
ISSN
0022-3263
Language
English

Subjects

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Residual Dipolar Couplings; Structural Discrimination; One Shot Measurements; https://purl.org/becyt/ford/1.3; https://purl.org/becyt/ford/1
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