Synthesis and Characterization of Ammonium Acesulfamate

Echeverría, Gustavo Alberto et al · Verlag Z Naturforsch · 2014

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Author / responsible party

Echeverría, Gustavo Alberto et al

Publisher

Verlag Z Naturforsch

Year

2014

ISSN

0932-0776

ISSN

0932-0776

Language

English

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Ammonium acesulfamate, (NH4)C4H4NO4S, was prepared by the reaction of acesulfamic acid and ammonium carbonate in aqueous solution, and characterized by elemental analysis and 1H and 13C NMR spectroscopy. Its crystal and molecular structure was determined by single-crystal X-ray diffraction methods. The substance crystallizes in the orthorhombic space group Pnma with Z = 4 molecules per unit cell. The NH4 + ion generates medium to strong hydrogen bonds with the carbonylic oxygen, the iminic nitrogen and the sulfonyl oxygen atoms of the acesulfamate anion. The FTIR spectrum of the compound was also recorded and is briefly discussed. Fil: Echeverría, Gustavo Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Instituto de Física La Plata. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Instituto de Física La Plata; Argentina Fil: Piro, Oscar Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Instituto de Física La Plata. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Instituto de Física La Plata; Argentina

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APA 7

Echeverría, G. A. E. A. (2014). Synthesis and Characterization of Ammonium Acesulfamate. http://hdl.handle.net/11336/24967

MLA

Echeverría, Gustavo Alberto et al. "Synthesis and Characterization of Ammonium Acesulfamate." 2014. http://hdl.handle.net/11336/24967.

Chicago

Echeverría, Gustavo Alberto et al. 2014. "Synthesis and Characterization of Ammonium Acesulfamate.". http://hdl.handle.net/11336/24967.

Harvard

Echeverría, G. A. E. A. 2014, Synthesis and Characterization of Ammonium Acesulfamate, Verlag Z Naturforsch, available at: http://hdl.handle.net/11336/24967 [Accessed 8 Aug. 2026].

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Title: Synthesis and Characterization of Ammonium Acesulfamate

Author / contributors: Echeverría, Gustavo Alberto et al

Publisher: Verlag Z Naturforsch

Publication year: 2014

ISSN: 0932-0776

ISSN: 0932-0776

Language: English

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Ammonium Acesulfamate; Synthesis; Crystal Structure; Ftir-Spectra; https://purl.org/becyt/ford/1.4; https://purl.org/becyt/ford/1